SPECTROSCOPY
ENVIRONMENT ANALYSIS
Faculty of Technology
Faculty of
Technology, Novi Sad, SCG
NIS-Refinery, Novi Sad, SCG
and University
of Dortmund (INFU), Dortmund, FRG
 |
 |
 INFU |
The
objective of the Summer school within the Center
for Applied Spectroscopy is to give advanced students in
chemistry practical instructions to conduct environmental analysis
according to the current state of art. We will focus on one specific group
of chemicals - the hydrocarbons - which are known to be a wide spread
contamination in soil and water due to industrial activities or unintended
spill. The oil refinery in Novi Sad was damaged heavily during the NATO
attacks in 1999 and as a result large quantities of petroleum, petroleum
derivatives and various burning products were released into the
environment. Within the course sampling, in situ measurements and the
analytical determination of hydrocarbons and PAH’s will be made in
cooperation with the Refinery and the Faculty of Technology of the
University of Novi Sad. During the workshop students will get a training
in sample preparation, sample clean up, quantification procedures and
method evaluation. In addition, lectures will be given to cover some of
the most important theoretical
aspects.
| Marinkovic-Neducin, Radmila | - University of Novi Sad, SCG |
| Marjanovic, Nikola | - University of Novi Sad, SCG |
| Pavlovic, Pavle | - Oil Refinery Novi Sad, SCG |
| Sinadinovic-Fiser, Snezana | - University of Novi Sad, SCG |
| Spiteller, Michael | - University of Dortmund, FRG |
University of Novi Sad
Faculty of Technology
Department of Petrochemical Engineering
Bul. Cara Lazara 1
21000 Novi Sad, SCG
Tel.: 381 (021) 450-288, 450-289
Fax: 381 (021) 450-413
E-mail: ssfiser@uns.ns.ac.yu
Sunday, 22. August | |
| – | Arrival, Check in |
| 19:00 – | REGISTRATION OF PARTICIPANTS |
| 19:30 – | Informal get together |
Monday, 23. August | |
| 08:00 – | Breakfast |
| 09:00 – | INTRODUCTION |
| 09:30 – | PETROLEUM PRODUCTS CONTAMINATION IN SOIL AND WATER IN OIL
REFINERY (Dipl. Ing. Pavle Pavlovic) (video tape, monitoring results, first remediation measures) |
| 10:30 – | INTRODUCTION TO SAFETY PRECAUTIONS |
| 11:00 – | Transportation to Refinery of Novi Sad |
| 11:30 – | ON SITE SAMPLING OF SOIL AND WATER FOR HYDROCARBONS AND
PAH’s |
| 13:00 – | Lunch |
| 14:00 – | PREPARATION OF THE SAMPLES FOR HYDROCARBONS AND PAH’s
ANALYSIS |
| 16:00 – | Transportation to Faculty of Technology |
Tuesday, 24. August | |
| 08:00 – | Breakfast |
| 09:00 – | INTRODUCTION TO GC/MS (Prof. Dr. Teodor Ast) |
| 10:30 – | EXTRACTION OF HYDROCARBONS FROM SOIL |
| 14:00 – | Lunch |
| 15:00 – | GC/MS ANALYSIS OF HYDROCARBONS IN SOIL |
| 18:00 – | Visit of the Fortress Petrovaradin |
Wednesday, 25. August | |
| 08:00 – | Breakfast |
| 09:00 – | GC/MS SAMPLE INLET SYSTEMS (Prof. Dr. Snezana Sinadinovic-Fisher) |
| 10:30 – | GC/MS ANALYSIS – IDENTIFICATION OF HYDROCARBONS IN SOIL |
| 13:00 – | Lunch |
| 14:00 – | EXTRACTION OF PAH`s FROM SOIL |
| 18:00 – | GC/MS ANALYSIS OF PAH`s IN SOIL |
Thursday, 26. August | |
| 08:00 – | Breakfast |
| 09:00 – | INTERPRETATION OF MASS SPECTRA (Prof. Dr. Michael
Spiteller) |
| 10:30 – | GC/MS ANALYSIS - DATA EVALUATION |
| 13:00 – | Lunch |
| 14:00 – | GC/MS ANALYSIS PAH’s – cont. |
| 20:00 – | Party at Danube |
Friday, 27. August | |
| 08:00 – | Breakfast |
| 09:00 – | WRITING THE REPORTS AND PREPARING PRESENTATIONS |
| 14:00 – | Lunch |
| 15:00 – | PRESENTATION OF REPORTS AND FINAL DISCUSSION |
Saturday, 28. August | |
| 09:00 – | VISIT OF THE MONASTERIES OF FRUSKA GORA |
| 14:00 – | Lunch |
| 17:00 – | RETURN FROM FRUSKA GORA |
Sunday, 29. August | |
| – | Leaving student guest house |